TA Instruments

AR1756-0012f

15/03/2013 15:14:15

Sample name	ASW Blank coupon#20 + DI + beads 50rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	12 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:14:15

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 50.00 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0120	49.80	-1240.4	10000	20.0	0.5624	1.012	-404.3	62.25	-6.495	2291	33.5198	0.5913	41.900	4190.0	3.411E-3	0.0	0.0
2.0240	50.00	36.075	10000	20.0	0.5563	2.024	11.76	62.49	0.1882	2267	83.7832	0.5804	104.73	10473	3.411E-3	0.0	0.0
3.0240	50.00	36.660	10000	20.0	0.5573	3.024	11.95	62.50	0.1912	2271	134.2340	0.5814	167.79	16779	3.411E-3	0.1	0.1
4.0240	50.00	36.783	10000	20.0	0.5559	4.024	11.99	62.50	0.1918	2265	184.6640	0.5799	230.83	23083	3.411E-3	0.1	0.1
5.0080	50.00	37.023	10000	20.0	0.5492	5.008	12.07	62.50	0.1931	2238	234.5770	0.5729	293.22	29322	3.411E-3	0.1	0.1
6.0080	50.00	36.771	10000	20.0	0.5500	6.008	11.99	62.50	0.1918	2241	284.8590	0.5737	356.07	35607	3.411E-3	0.1	0.1
7.0080	50.00	36.939	10000	20.0	0.5486	7.008	12.04	62.50	0.1926	2235	335.1340	0.5722	418.92	41892	3.411E-3	0.1	0.1
8.0080	50.00	37.065	10000	20.0	0.5492	8.008	12.08	62.50	0.1933	2238	385.4030	0.5729	481.75	48175	3.411E-3	0.1	0.1
9.0320	50.00	36.974	10000	20.0	0.5462	9.032	12.05	62.50	0.1928	2225	435.6330	0.5697	544.54	54454	3.411E-3	0.2	0.2
10.012	50.00	37.136	10000	20.0	0.5442	10.012	12.10	62.50	0.1937	2217	485.9080	0.5676	607.39	60739	3.411E-3	0.2	0.2
11.024	50.00	36.738	10000	20.0	0.5431	11.024	11.97	62.50	0.1916	2213	536.4450	0.5665	670.56	67056	3.411E-3	0.2	0.2
12.024	50.00	36.855	10000	20.0	0.5395	12.024	12.01	62.50	0.1922	2198	586.4520	0.5627	733.07	73307	3.411E-3	0.2	0.2
13.012	50.00	37.306	10000	20.0	0.5399	13.012	12.16	62.50	0.1946	2200	636.6950	0.5631	795.87	79587	3.411E-3	0.2	0.2
14.008	50.00	36.939	10000	20.0	0.5409	14.008	12.04	62.50	0.1926	2204	687.1630	0.5642	858.95	85895	3.411E-3	0.2	0.2
15.024	50.00	36.577	10000	20.0	0.5403	15.024	11.92	62.50	0.1908	2201	737.2750	0.5635	921.59	92159	3.411E-3	0.3	0.3
16.024	50.00	35.823	10000	20.0	0.5362	16.024	11.68	62.50	0.1868	2185	787.5120	0.5593	984.39	98439	3.411E-3	0.3	0.3
17.052	50.00	36.054	10000	20.0	0.5348	17.052	11.75	62.50	0.1880	2179	838.4070	0.5578	1048.0	1.0480E5	3.411E-3	0.3	0.3
18.024	50.00	35.911	10000	20.0	0.5330	18.024	11.71	62.50	0.1873	2172	890.8680	0.5559	1113.6	1.1136E5	3.411E-3	0.3	0.3
19.012	50.00	36.298	10000	20.0	0.5326	19.012	11.83	62.50	0.1893	2170	938.9000	0.5555	1173.6	1.1736E5	3.411E-3	0.3	0.3
20.008	50.00	36.938	10000	20.0	0.5360	20.008	12.04	62.50	0.1926	2184	988.6030	0.5591	1235.8	1.2358E5	3.411E-3	0.3	0.3
21.024	50.00	36.314	10000	20.0	0.5338	21.024	11.84	62.50	0.1894	2175	1039.0300	0.5568	1298.8	1.2988E5	3.411E-3	0.4	0.4
22.024	50.00	36.649	10000	20.0	0.5289	22.024	11.95	62.50	0.1911	2155	1089.4600	0.5517	1361.8	1.3618E5	3.411E-3	0.4	0.4
23.008	50.00	36.104	10000	20.0	0.5289	23.008	11.77	62.50	0.1883	2155	1139.5900	0.5517	1424.5	1.4245E5	3.411E-3	0.4	0.4
24.012	50.00	36.272	10000	20.0	0.5312	24.012	11.82	62.50	0.1892	2164	1190.0601	0.5540	1487.6	1.4876E5	3.411E-3	0.4	0.4
25.008	50.00	36.275	10000	20.0	0.5271	25.008	11.82	62.50	0.1892	2148	1240.1300	0.5498	1550.2	1.5502E5	3.411E-3	0.4	0.4
26.008	50.00	35.938	10000	20.0	0.5275	26.008	11.71	62.50	0.1874	2149	1290.8700	0.5502	1613.6	1.6136E5	3.411E-3	0.4	0.4
27.024	50.00	36.103	10000	20.0	0.5269	27.024	11.77	62.50	0.1883	2147	1340.8400	0.5496	1676.1	1.6761E5	3.411E-3	0.5	0.5
28.008	50.00	35.677	10000	20.0	0.5267	28.008	11.63	62.50	0.1861	2146	1390.9301	0.5494	1738.7	1.7387E5	3.411E-3	0.5	0.5
29.008	50.00	36.475	10000	20.0	0.5281	29.008	11.89	62.50	0.1902	2152	1441.3199	0.5509	1801.7	1.8017E5	3.411E-3	0.5	0.5
30.008	50.00	35.994	10000	20.0	0.5237	30.008	11.73	62.50	0.1877	2134	1491.5500	0.5462	1864.4	1.8644E5	3.411E-3	0.5	0.5
31.024	50.00	35.678	10000	20.0	0.5239	31.024	11.63	62.50	0.1861	2134	1542.0100	0.5464	1927.5	1.9275E5	3.411E-3	0.5	0.5
32.008	50.00	35.679	10000	20.0	0.5224	32.008	11.63	62.50	0.1861	2129	1592.2000	0.5449	1990.3	1.9903E5	3.411E-3	0.5	0.5
33.024	50.00	35.367	10000	20.0	0.5200	33.024	11.53	62.50	0.1844	2119	1642.1899	0.5424	2052.7	2.0527E5	3.411E-3	0.6	0.6
34.028	50.00	35.650	10000	20.0	0.5216	34.028	11.62	62.50	0.1859	2125	1692.6500	0.5441	2115.8	2.1158E5	3.411E-3	0.6	0.6
35.008	50.00	36.076	10000	20.0	0.5200	35.008	11.76	62.50	0.1881	2119	1742.9100	0.5424	2178.6	2.1786E5	3.411E-3	0.6	0.6
36.012	50.00	36.349	10000	20.0	0.5231	36.012	11.85	62.50	0.1896	2131	1793.1000	0.5456	2241.4	2.2414E5	3.411E-3	0.6	0.6
37.024	50.00	36.356	10000	20.0	0.5216	37.024	11.85	62.50	0.1896	2125	1843.2500	0.5441	2304.1	2.3041E5	3.411E-3	0.6	0.6
38.008	50.00	36.111	10000	20.0	0.5243	38.008	11.77	62.50	0.1883	2136	1893.3500	0.5468	2366.7	2.3667E5	3.411E-3	0.6	0.6
39.028	50.00	36.192	10000	20.0	0.5192	39.028	11.80	62.50	0.1887	2115	1944.1100	0.5415	2430.1	2.4301E5	3.411E-3	0.7	0.7
40.024	50.00	35.777	10000	20.0	0.5186	40.024	11.66	62.50	0.1866	2113	1993.9200	0.5409	2492.4	2.4924E5	3.411E-3	0.7	0.7
41.024	50.00	36.132	10000	20.0	0.5188	41.024	11.78	62.50	0.1884	2114	2044.1500	0.5411	2555.2	2.5552E5	3.411E-3	0.7	0.7
42.024	50.00	35.923	10000	20.0	0.5196	42.024	11.71	62.50	0.1873	2117	2094.4700	0.5420	2618.1	2.6181E5	3.411E-3	0.7	0.7
43.008	50.00	35.948	10000	20.0	0.5182	43.008	11.72	62.50	0.1875	2111	2144.6699	0.5405	2680.8	2.6808E5	3.411E-3	0.7	0.7
44.024	50.00	35.997	10000	20.0	0.5151	44.024	11.73	62.50	0.1877	2099	2194.9700	0.5373	2743.7	2.7437E5	3.411E-3	0.7	0.7
45.012	50.00	35.791	10000	20.0	0.5137	45.012	11.67	62.50	0.1867	2093	2245.2000	0.5358	2806.5	2.8065E5	3.411E-3	0.8	0.8
46.008	50.00	35.734	10000	20.0	0.5155	46.008	11.65	62.50	0.1864	2101	2295.5000	0.5377	2869.4	2.8694E5	3.411E-3	0.8	0.8
47.008	50.00	36.509	10000	20.0	0.5121	47.008	11.90	62.50	0.1904	2086	2345.7800	0.5341	2932.2	2.9322E5	3.411E-3	0.8	0.8
48.008	50.00	35.975	10000	20.0	0.5097	48.008	11.73	62.50	0.1876	2077	2395.9800	0.5316	2995.0	2.9950E5	3.411E-3	0.8	0.8
49.012	50.00	36.398	10000	20.0	0.5086	49.012	11.86	62.50	0.1898	2072	2446.2800	0.5305	3057.9	3.0579E5	3.411E-3	0.8	0.8
50.008	50.00	35.549	10000	20.0	0.5111	50.008	11.59	62.50	0.1854	2082	2496.7500	0.5331	3120.9	3.1209E5	3.411E-3	0.8	0.8
51.028	50.00	35.962	10000	20.0	0.5076	51.028	11.72	62.50	0.1875	2068	2546.7900	0.5295	3183.5	3.1835E5	3.411E-3	0.9	0.9
52.024	50.00	36.170	10000	20.0	0.5119	52.024	11.79	62.50	0.1886	2086	2597.0601	0.5339	3246.3	3.2463E5	3.411E-3	0.9	0.9
53.024	50.00	36.347	10000	20.0	0.5115	53.024	11.85	62.50	0.1896	2084	2647.7200	0.5335	3309.7	3.3097E5	3.411E-3	0.9	0.9
54.028	50.00	36.251	10000	20.0	0.5137	54.028	11.82	62.50	0.1891	2093	2697.6201	0.5358	3372.0	3.3720E5	3.411E-3	0.9	0.9
55.008	50.00	36.038	10000	20.0	0.5070	55.008	11.75	62.50	0.1879	2066	2747.8899	0.5288	3434.9	3.4349E5	3.411E-3	0.9	0.9
56.032	50.00	35.862	10000	20.0	0.5103	56.032	11.69	62.50	0.1870	2079	2798.1699	0.5322	3497.7	3.4977E5	3.411E-3	0.9	0.9
57.008	50.00	36.195	10000	20.0	0.5080	57.008	11.80	62.50	0.1888	2070	2848.6201	0.5299	3560.8	3.5608E5	3.411E-3	1.0	1.0
58.024	50.00	36.014	10000	20.0	0.5170	58.024	11.74	62.50	0.1878	2106	2899.8401	0.5392	3624.8	3.6248E5	3.411E-3	1.0	1.0
59.024	50.00	36.036	10000	20.0	0.4993	59.024	11.75	62.50	0.1879	2034	2949.4299	0.5208	3686.8	3.6868E5	3.411E-3	1.0	1.0
60.024	50.00	37.036	10000	20.0	0.5129	60.024	12.07	62.50	0.1932	2090	3000.2100	0.5350	3750.3	3.7503E5	3.411E-3	1.0	1.0

